Re: HPLC of refolded proteins

From: Roger Murphy (Roger.Murphy@ludwig.edu.au)
Date: Mon Sep 18 2000 - 18:13:05 EDT


Dirk,

I've routinely used shots (up to 1ml at a time) of 6M guanidine HCl as
restoratives for C18 columns that have seen too much garbage from tissue
extracts. Doesn't harm the column at all.

Roger

At 05:23 PM 9/18/00 +0100, J.betley wrote:
>Dear All,
>
>Does anyone have experience of HPLC of proteins in refold buffers? The
>protein samples contain things such as strong urea and guanidine; we
>wonder what effect this would have on, for example, RP18 HPLC columns. If
>this is a no-no, then are there any suggestions as to alternatives?
>
>Thanks
>
>Dirk



This archive was generated by hypermail 2b29 : Wed Sep 20 2000 - 11:12:13 EDT