Dear Michael:
In addition to the reference given by Daniel Wellner I recommend to
look through the chapter on the synthesis of homooligopeptides in
"Synthese von Peptiden. (Muller, E. Ed.) In: Houben Weil's Methoden der
Organichen Chemie, Stuttgart: Thieme 1974, Bd.15, Teil 1-2."
You will also find few representative experimental procedures there.
Regards,
Igor Rodionov
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