Re: Pseq Prolines

Jacek_Mozdzanowski-1@SBPHRD.com
Thu, 18 Sep 1997 08:05:54 -0400

To: abrf@aecom.yu.edu
cc:
From: Jacek Mozdzanowski-1 @ SB_PHARM_RD
Date: 18-Sep-97 01:05:54 PM
Subject: Re: Pseq Prolines
Categories:

Deb,
My understanding is that the sequence is known. In such a case the best
approach is to "custom craft" sequencing cycles. Longer cleavage time is
necessary for proline and shorter time for all the other residues.
Switching to the gas phase could be helpful, too. With this approach you
should be able to improve the lag (carryover) and reduce the washout quite
a bit. Check: W.H.Vensel, D.D.Kasarda, Techniques in Protein Chemistry II,
pp 181-190.

Jacek Mozdzanowski
Analytical Sciences
SmithKline Beecham